Vidyantari, Lyra (2025) PEMANFAATAN LIMBAH KACA DALAM PEMBUATAN SILIKA GEL MENGGUNAKAN NATRIUM HIDROKSIDA (NaOH) DENGAN METODE SOL GEL. Undergraduate thesis, UPN Veteran Jawa Timur.
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Abstract
The utilization of glass waste as raw material for silica gel is carried out using the sol-gel method to produce high-quality products while reducing inorganic waste. Silica is extracted from glass waste using sodium hydroxide (NaOH), then converted into sodium silicate. Silica gel synthesis is carried out by varying two main parameters: the sodium silicate:water ratio (1:1, 1:2, 1:3, 1:4, and 1:5) and sulfuric acid concentration (1.5 M; 2 M; 2.5 M; 3 M; and 3.5 M). Product characterization was performed using XRF for SiO₂ content, XRD for amorphous structure, and BET for specific surface area. The highest SiO₂ content of 86.83% was obtained at a ratio of 1:5 and H₂SO₄ concentration of 3.5 M, while the highest specific surface area of 186.82 m²/g was achieved at the same ratio and 3 M. Optimization using the Response Surface Methodology (RSM) indicated theoretical optimum conditions at a ratio of 1:10 and H₂SO₄ concentration of 7.27 M. These conditions highlight the balance between sufficient acid strength to remove metallic and organic impurities and adequate dilution to maintain effective mass transfer, resulting in a SiO₂ purity of up to 99%. These results highlight the high potential of glass waste as an alternative silica source for adsorbent and catalyst support applications.
| Item Type: | Thesis (Undergraduate) | ||||||||
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| Subjects: | T Technology > TP Chemical technology T Technology > TP Chemical technology > TP155 Chemical engineering |
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| Divisions: | Faculty of Engineering > Departement of Chemical Engineering | ||||||||
| Depositing User: | Lyra Vidyan Tari | ||||||||
| Date Deposited: | 04 Nov 2025 05:07 | ||||||||
| Last Modified: | 04 Nov 2025 05:07 | ||||||||
| URI: | https://repository.upnjatim.ac.id/id/eprint/46086 |
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