Sintesis dan Pemurnian Kalsium Hidroksida (Ca(OH)2) dari Limbah Karbit Industri Asetilena Melalui Metode Pelarutan dan Presipitasi

Gustika, Cinta Ananda (2026) Sintesis dan Pemurnian Kalsium Hidroksida (Ca(OH)2) dari Limbah Karbit Industri Asetilena Melalui Metode Pelarutan dan Presipitasi. Undergraduate thesis, UPN Veteran jawa Timur.

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Abstract

The increasing production of acetylene gas generates large amounts of carbide waste, which may cause environmental problems if not properly managed. This study aims to utilize carbide waste as a raw material for the synthesis and purification of calcium hydroxide (Ca(OH)₂) through a dissolution–precipitation method. Hydrochloric acid (HCl) was used in the dissolution stage to dissolve calcium compounds, while sodium hydroxide (NaOH) was used in the precipitation stage to recover Ca(OH)₂ with higher purity. The effects of HCl concentration (1.5–3.5 N) and extraction temperature (35–55°C) were investigated to determine the optimum operating conditions. The synthesized products were subsequently characterized using X-Ray Fluorescence (XRF) and Fourier Transform Infrared Spectroscopy (FTIR). The results showed that increasing the HCl concentration and extraction temperature generally increased the Ca(OH)₂ yield, with the optimum conditions achieved at an HCl concentration of 3.5 N and an extraction temperature of 50°C, resulting in the highest yield of 57.07%. XRF analysis indicated that the calcium content in the final product remained high, reaching 98–99%, demonstrating the effectiveness of the purification process. FTIR characterization confirmed the presence of hydroxyl (–OH) groups, which are characteristic of Ca(OH)₂, at a wavenumber of approximately 3640 cm⁻¹. These findings demonstrate that the dissolution–precipitation method is effective for converting carbide waste into high-purity calcium hydroxide, while supporting waste valorization and environmentally friendly industrial waste management.

Item Type: Thesis (Undergraduate)
Contributors:
ContributionContributorsNIDN/NIDKEmail
Thesis advisorSanti, Sintha SorayaNIDN0021066609sintha.tk@upnjatim.ac.id.
Subjects: T Technology > TP Chemical technology > TP155 Chemical engineering
Divisions: Faculty of Engineering > Departement of Chemical Engineering
Depositing User: Cinta Ananda Gustika
Date Deposited: 13 Oct 2026 03:25
Last Modified: 13 Oct 2026 07:40
URI: https://repository.upnjatim.ac.id/id/eprint/60652

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