Pra Rancangan Pabrik Asam Sulfamat dari Urea dan Oleum dengan Proses Sulfonasi

Djunaidy, Natasya Salsabila Putri (2025) Pra Rancangan Pabrik Asam Sulfamat dari Urea dan Oleum dengan Proses Sulfonasi. Undergraduate thesis, UPN Veteran Jawa Timur.

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Abstract

A Sulfamate Acid Plant from Urea and Oleum will be established in the JIIPE Industrial Area, Gresik. The main raw materials are Oleum (H₂SO₄·SO₃) and Urea (CO(NH₂)₂). The Sulfamate Acid production process consists of three stages. The first stage is the pre-treatment of raw materials, where Oleum is heated to 60°C to match the reactor’s operating temperature. The second stage is sulfonation process between Oleum and Urea, producing Sulfamate Acid and Carbon Dioxide (CO₂). The CO₂ gas is immediately separated into a storage tank for subsequent sale to third parties. This reaction process achieves a conversion rate of 90%. The third stage is purification, where crude Sulfamate Acid from the reactor is transferred to a crystallizer using sodium sulfate as a solvent, separated by a centrifuge, and dissolved again in a dissolving tank. The solution undergoes recrystallization using ethanol to enhance purity and is again separated via centrifuge. The resulting solid product is dried using a rotary dryer, cooled with a cooling conveyor, and finally transported to a silo for storage and packaging. The plant’s electricity will be supplied by PLN and a generator set, while water will be sourced from the nearby Bengawan Solo River. The plant will operate under a limited liability company (PT) structure, employing a line-and-staff organization system. The facility is designed for continuous operation with a production schedule of 330 days per year.

Item Type: Thesis (Undergraduate)
Contributors:
ContributionContributorsNIDN/NIDKEmail
Thesis advisorMuljani, SrieNIDN0012116111sriemuljani.tk@upnjatim.ac.id
Subjects: T Technology > TP Chemical technology > TP155 Chemical engineering
Divisions: Faculty of Engineering > Departement of Chemical Engineering
Depositing User: Natasya Salsabila Putri
Date Deposited: 03 Dec 2025 07:46
Last Modified: 03 Dec 2025 08:50
URI: https://repository.upnjatim.ac.id/id/eprint/47548

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